**篇 基礎(chǔ)化學(xué)實(shí)驗(yàn)基本知識(shí)**章 實(shí)驗(yàn)室規(guī)則及安全知識(shí) 1.基礎(chǔ)化學(xué)實(shí)驗(yàn)?zāi)康? 2.化學(xué)實(shí)驗(yàn)室一般規(guī)則 3.化學(xué)實(shí)驗(yàn)室的安全知識(shí) 4.化學(xué)實(shí)驗(yàn)操作過程中可能發(fā)生的事故與處理 5.化學(xué)實(shí)驗(yàn)室的防火、防電與滅火常識(shí)第二章 基礎(chǔ)化學(xué)實(shí)驗(yàn)常用儀器 1.實(shí)驗(yàn)室常用儀器介紹 2.玻璃儀器的洗滌和干燥 3.常用儀器使用方法第三章 實(shí)驗(yàn)結(jié)果的表示 1.實(shí)驗(yàn)誤差與有效數(shù)字 2.實(shí)驗(yàn)數(shù)據(jù)的處理 3.實(shí)驗(yàn)報(bào)告第二篇 基礎(chǔ)化學(xué)實(shí)驗(yàn)課題 實(shí)驗(yàn)課題一 基本操作訓(xùn)練實(shí)驗(yàn) 實(shí)驗(yàn)一 常用容量分析儀器操作練習(xí) 實(shí)驗(yàn)二 電子天平稱量練習(xí) 實(shí)驗(yàn)三 緩沖溶液的配制與性質(zhì)、溶液pH測(cè)定 實(shí)驗(yàn)四 膠體溶液的制備與性質(zhì) 實(shí)驗(yàn)課題二 滴定分析實(shí)驗(yàn) 實(shí)驗(yàn)五酸堿滴定分析法 1.標(biāo)準(zhǔn)鹽酸溶液濃度的標(biāo)定 2.標(biāo)準(zhǔn)氫氧化鈉溶液濃度的標(biāo)定 3.食用醋中總酸度的測(cè)定 4.硼砂含量的測(cè)定 5.返滴定法測(cè)定阿司匹林的含量 實(shí)驗(yàn)六 氧化還原滴定法 1.高錳酸鉀法 2.碘量法 實(shí)驗(yàn)七 配位滴定分析 1.水的硬度的測(cè)定 2.明礬含量的測(cè)定 3.葡萄糖酸鈣含量的測(cè)定 實(shí)驗(yàn)課題三 分光光度法實(shí)驗(yàn) 實(shí)驗(yàn)八 可見分光光度法測(cè)定水樣中鐵含量 1.鄰二 氮菲法 2.硫氰酸鹽法 3.磺基水楊酸法 實(shí)驗(yàn)九 分光光度法測(cè)定阿司匹林藥片的含量 實(shí)驗(yàn)十 分光光度法測(cè)定磺基水楊酸合鐵的組成和穩(wěn)定常數(shù) 實(shí)驗(yàn)十一 熒光分析法測(cè)定維生素B2的含量 實(shí)驗(yàn)十二 紫外分光光度法對(duì)維生素B12的鑒別與含量測(cè)定 實(shí)驗(yàn)課題四 化學(xué)原理實(shí)驗(yàn) 實(shí)驗(yàn)十三 稀溶液的依數(shù)性及其應(yīng)用 1.凝固點(diǎn)降低法測(cè)定溶質(zhì)的分子量 2.利用溶液的滲透濃度測(cè)定溶質(zhì)的相對(duì)分子質(zhì)量 3.冰點(diǎn)滲透壓計(jì)的應(yīng)用 實(shí)驗(yàn)十四 置換法測(cè)定鎂的原子量 實(shí)驗(yàn)十五 化學(xué)反應(yīng)速率與活化能的測(cè)定 實(shí)驗(yàn)十六 *大氣泡壓力法測(cè)定乙醇溶液的表面張力 實(shí)驗(yàn)課題五 化合物制備實(shí)驗(yàn) 實(shí)驗(yàn)十七 氯化鈉的精制 實(shí)驗(yàn)十八 硫酸亞鐵銨的制備 實(shí)驗(yàn)十九 轉(zhuǎn)化法制備硝酸鉀 實(shí)驗(yàn)課題六 綜合及研究性實(shí)驗(yàn) 實(shí)驗(yàn)二十 醋酸解離常數(shù)的測(cè)定與食醋中HAc含量的測(cè)定 實(shí)驗(yàn)二十一 茶葉中鈣、鎂及鐵含量的測(cè)定 實(shí)驗(yàn)課題七 自行設(shè)計(jì)實(shí)驗(yàn) 實(shí)驗(yàn)二十二 實(shí)驗(yàn)設(shè)計(jì)及研究 Part Ⅰ Experiment Essentials in Basic Chemistry Chapter l Laboratory Rules and Safety Information 1. The Purpose of Experiments in Basic Chemistry 2. General Rules in Laboratory 3. Safety Information 4. The Treatment of Accidents in Chemical Experiments 5. Fire Prevention, Anti-electricity and Extinguishing Knowledge Chapter 2 Ordinary Instruments in Chemical Experiments 1. Introduction of Ordinary Instruments in Chemical Laboratory 2. Cleaning and Drying Glasswares 3. Operation of Instrument Chapter 3 Experiment Results and their Expressions 1. Experimental Error and Significant Figures 2. Treatments of Experimental Data 3. Experiment Reports Part Ⅱ Experiments in Basic Chemistry Chapter 1 Experiments of Basic Operation Practice Experiment 1 Operation of Volumetric Analysis Experiment 2 Weighing Practice with an Electronic Balance Experiment 3 Preparation, Properties and pH Measurement of Buffer Solutions Experiment 4 Preparation and Properties of Colloidal Systems Chapter 2 Experiments of Titration Analysis Experiment 5 Acid-Base Titration Analysis 1. Standardization of the Concentration of HCI Solution 2. Standardization of the Concentration of NaOH Solution 3. Determination of Acetic Acid Content in Vinegar 4. Determination of Borax Content 5. Determination of Aspirin Content by Back Titration Experiment 6 Oxidation-Reduction Titration 1. Potassium Permanganate Method 2. lodimetry Experiment 7 Complexometric Titration 1. Determination of Water Hardness 2. Determination of KAl(SO4)2·12H2O in Alum 3. Determination of Calcium Gluconate Chapter 3 Spectrophotometry Experiment 8 Determination of Fe3+ (Fe2+) Content in Water Sample with Visible Spectrophotometry 1. O-phenanthroline Method 2. Sulfocyanate Method 3. Sulfosalicylic Acid Method Experiment 9 Determination of Aspirin Content in Tablets by Visible Spectrophotometry Experiment 10 Determination of the Formula and the Stability Constant of Sulfosalicylate Iron (Ⅲ) by Spectrophotometry Experiment 11 Determination of Vitamin B2 by Fluorescence Analysis Experiment 12 Identification and Content Determination of Vitamin B12 by Ultraviolet Spectrophotometry Chapter 4 Chemical Principles Experiment Experiment 13 Colligative Properties of Dilute Solution and Their Application 1. Determination of Molar Mass of Glucose by Freezing Point Depression 2. Determination of the Molar Mass of Glucose by Determining Osmolarity 3. Application of Freezing Point Osmometer Experiment 14 Determination of the Relative Atomic Mass of Magnesium by Replacement Reaction Experiment 15 Determination of the Rate of Chemical Reaction and Activation Energy Experiment 16 The Maximum Bubble Pressure Method to Determine the Surface Tension of Ethanol Solution Chapter 5 Preparation of Compounds Experiment 17 Refining Sodium Chloride Experiment 18 Preparation of Ammonium Iron (U) Sulfate Experiment 19 Preparation of Potassium Nitrate by Conversion Method Chapter 6 Comprehensive Experiments Experiment 20 Determination of HAc Content and Dissociation Equilibrium Constant of Content of HAc Experiment 21 Determination of the Content of Calcium, Magnesium, and Iron in Tea Chapter 7 Self-Designed Experiment Experiment 22 Design and Research附錄 附錄Ⅰ 國際相對(duì)原子量表 附錄Ⅱ 不同溫度下水的飽和蒸汽壓 附錄Ⅲ 危險(xiǎn)藥品的分類、性質(zhì)和管理 附錄Ⅳ 標(biāo)準(zhǔn)緩沖溶液 附錄Ⅴ 參考書目