**章 一般性實驗指導chapter 1 general instructions **節 實驗室安全守則 section 1 laboratory safety 第二節 天平使用規程 section 2 protocol for using balance 第三節 有效數字的修約 section 3 rounding of significant figures 第四節 一般性規定一 section 4 general noices 第五節 實驗記錄及報告格式 section 5 experiment record and report format第二章 藥物的性狀、鑒別和檢查chapter 2 description,identification and tests of drugs 實驗一 葡萄糖的性狀、鑒別和檢查一 experiment 1 description,identification and tests of glucose 實驗二 乙酸氫化可的松或乙酸氫化可的松片的鑒別和檢查 experiment 2 description,identification and tests of hydrocortisone acetate or hydrocortisone acetate tablets。 實驗三 甲苯咪唑的性狀、鑒別和檢查 experiment 3 description,identification and tests of mebendazole 實驗四 典型中藥的鑒別 experiment 4 description,identification and test of typical tcm第三章 藥物的含量測定chapter 3 determination of drugs 實驗五 硫酸奎尼丁及其片劑的含量測定 experiment 5 assay of quinidine sulfate and quinidine s111fl爿tp tablpts 實驗六 鹽酸普魯卡因或注射用鹽酸普魯卡因的含量測定 experiment 6 assay of procaine hydrochloride or procaine hydrochloride for injection 實驗七 碘苯酯及其注射液的含量測定 experiment 7 assay of iophendylate and iophendylate injection 實驗八 頭孢拉定及其片劑的含量測定 experiment 8 assay of cefradine and cefradine tablets 第四章 藥物質量的全檢驗 chapter 4 drug analysis 實驗九 維生素e或維生素e軟膠囊的質量檢查 experiment 9 analysis of vitamin e and vitamin e soft capsules 實驗十 阿司匹林與阿司匹林腸溶片的質量分析 experiment 10 analysis of aspirin and aspirin enteric.coated tablets 實驗十一 復方磺胺甲惡唑片的質量分析 experiment 1 1 analysis of compound sulfamethoxazole tablets 實驗十二 頭孢克洛或頭孢克洛膠囊的質量分析 experiment 1 2 analysis of cefaclor or cefaclor capsules 實驗十三 石菖蒲的質量檢驗 experiment 1 3 analysis of acori talarinowii rhizoma 實驗十四 六味地黃丸的質量檢驗 experiment 14 analysis of liuwei dihuang wan 實驗十五 雙黃連口服液的質量檢驗 expenment 15 analysis of shuanghuanglian koufuye第五章 生物樣本中藥物的分析chapter 5 q,mntitation of drugs in biological matrix 實驗十六 兔血清中茶堿的高效液相色譜法測定 experiment 16 determination of theophylline in rabbit,s serum by hplc 實驗十七 阿司匹林代謝產物水楊酸的血漿濃度測定 experiment 17 determination of salicylic acid(sa),metabolite of aspirin(asa)in humans plasma by hplc 實驗十八 高效液相色譜法測定尿液中苯巴比妥的濃度 experiment 18 determination of phenobarbital in human,s urine by hplc 實驗十九 lc—ms/ms法測定比格犬血漿中阿奇霉素的含量 experiment 19 determination of azithromycin in beagle,s plasma by lc——ms/ms第六章設計類實驗 chapter 6 designing experiment 實驗二十 蘭索拉唑的鑒別實驗 experiment 20 identification of lansoprazole 實驗二十一 蘭索拉唑的雜質檢查實驗 experiment 21 examination for impurities in lansoprazole 實驗二十二 蘭索拉唑的含量測定實驗 experiment 22 content determination of lansoprazole 實驗二十三 酮康唑的血藥濃度測定 experiment 23 determination of ketoconazole concentration in plasma 實驗二十四 清開靈口服液的質量分析 experiment 24 analysis of qingkailing koufuye 第七章 分析方法驗證chapter 7 validation 0f analysis method 一、藥品質量標準分析方法驗證指導原則 二、生物樣品分析方法的基本要求 1.a guideline for the validation of analytical method adopted in pharmaceutical 2.the basic requirements for analytical methods of biological specimen附錄 實驗室常用英語appendix laboratory commonly used in english